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Centrifuge the viral supernatant at 1,140 x g for 10 min at 4 °C to clear up cell debris from the supernatant. Transfer cleared supernatant to 50 ml tube and store at 4 °C. NOTE: Day 5: At 72 hr post-transfection, collect the second batch of viral supernatant. Repeat step 2.3.1 and pool 48 and 72 hr cleared supernatants.
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After 40 h. only a 4490 conversion of (Z)-2-pentene is achieved (molar ratio: alkene[W = 80 - 100/1_ 2' = 298 K) [181 _ No catalytic activity remained after such a long period of time. hi comparison, systems such as W(CO)5L/EtAlC12/02 (L = CO, P(Ph)3, P(OPh)3) convert 2-pentene within. 25 min into an equilibrium nixture of 2-butene and 3-hegene ...
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To collect a native high-resolution dataset from a second crystal originating from the same crystallization condition set up the wavelength of the beam to 1.00 Å (12,398 keV). Collect data at 100 K. The exposure time is 0.1 sec with 0.1° rotation per image. Set the transmission to 70% (0.7). 5. Structure Determination via Zinc-SAD
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At 70 °C with oil:methanol:acid molar ratios of 1:245:3.8, and at 80 °C with oil:methanol:acid molar ratios in the range 1:74:1.9–1:245:3.8, the transesterification was essentially a pseudo ...
A method for delignifying ligno-cellulosic materials and efficiently separate from each other the constituents thereof. Said materials which optionally may be prehydrolized are heated in an aqueous acid medium in the presence of phenol compounds whereby the ratio by weight of liquid to solid is at least 0,5. In the case of low liquid solid ratios i.e. below about 4:1 further aqueous liquid is ...
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The resonance forms X and XI, involving an allylic shift, makes possible the recombination of carbon 8 with either oarbon 2 or 6 to form dor 1-alpha pinene. The forma X and XI, and also VIII and XII, are mirror images, and hence represent optical isomers. This accounts for the decrease in optical activity noted by Fuguitt and Hawkins (15).
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